Sampling

Statuspapier Mikroplastik-Analytik

hannes.schritt@ecologic.eu — Mon, 28 Jun 2021 13:22:16 +0000

Analysis of Microplastics - Sampling, preparation and detection methods hannes.schritt… Mon, 06/28/2021 - 15:22

Untertitel

Status Report

Titelbild

Beschreibung

This status report was prepared within the framework of the cross-cutting topic 1 "Analytics and reference materials" of the research focus. It summarizes the contents of the project discussions and coordination within the cross-cutting issue. The organization of this ongoing process of development or elaboration has been supported by several events.

The status report presents a summary of the physicochemical methods for the analysis of MP used in the research focus "Plastics in the Environment". The present recommendations are based on the current state of knowledge of the analysis of MP and are directed at actors in science as well as potential users in practice.

Scientists from the following collaborative projects of the research focus participated in the preparation of the status report via workshops, contributions and feedback loops: EmiStop, ENSURE, MicBin, MicroCatch_Balt, MikroPlaTaS, PLASTRAT, PLAWES, RAU, REPLAWA, RUSEKU, SubμTrack and TextileMission as well as the two predecessor projects MiWa and BASEMAN.

Further Links

Link to Status Report

Year

2020

Type of Result

discussion papers & status papers

Citation

Braun, Ulrike & Stein, Ulf & Schritt, Hannes & Altmann, Korinna & Bannick, Claus & Becker, Roland & Bitter, Hajo & Bochow, Mathias & Dierkes, Georg & Enders, Kristina & Eslahian, Kyriakos & Fischer, Dieter & Földi, Corinna & Fuchs, Monika & Gerdts, Gunnar & Hagendorf, Christian & Heller, Claudia & Ivleva, Natalia & Jekel, Martin & Kerpen, Jutta & Klaeger, Fraziska & Knoop, Oliver & Labrenz, Matthias & Laforsch, Christian & Obermaier, Nathan & Primpke, Sebastian & Reiber, Jens & Richter, Susanne & Ricking, Mathias & Scholz-Böttcher, Barbara & Stock, Friederike & Wagner, Stephan & Wendt-Potthoff, Katrin & Zumbülte, Nicole (2021): Analysis of Microplastics - Sampling, preparation and detection methods. Status Report within the framework program Plastics in the Environment.

Tags

Sewage

Analytics

Sampling

Soil

Raman microspectroscopy

Publikationstyp

Factsheet 11: Mikroplastik in der Abwasserbehandlung - Methodenentwicklung für Probenahme und Analyse zur Erfassung der Eintragsmengen in Oberflächengewässer

janna.vakili@ecologic.eu — Thu, 06 May 2021 12:46:43 +0000

Factsheet 11: Microplastics in wastewater treatment - Development of sampling and analysis methods for detection of input quantities into surface waters janna.vakili@e… Thu, 05/06/2021 - 14:46

Titelbild

Photo: © Institute of Hydroscience, University of the Federal Armed Forces Munich

Beschreibung

It is not easy to determine how much microplastic is contained in wastewater and sewage sludge. In addition to plastic, countless other particles and substances are present. To reliably determine the concentration of microplastic particles, complex procedures for sampling as well as for removal of foreign substances and analysis of the microplastic particles are required.

The PLASTRAT research team has set itself the task of developing methods for these procedures and thus advancing the detection of inputs to surface waters. In this context, they provide important insights into the relevance of wastewater treatment plants as a retention option for plastic particles.

The project focuses on the quantification and technical reduction potential of plastic emissions in the field of urban water management, including sewage sludge treatment. The results on method development have been summarized in the 11th fact sheet of the research focus. The fact sheet is available for PDF download here.

Attachments

Factsheet 11 of the BMBF Research Focus Plastics in the Environment.

Joint project

PLASTRAT

Year

2021

Author

Authors

Natalie Wick

Steffen Krause

Christian Schaum

Franziska Fischer

Dieter Fischer

Franziska Klaeger

Juliana Ivar do Sul

Matthias Labrenz

Type of Result

factsheets

Citation

Wick, Natalie; Krause, Steffen; Schaum, Christian; Fischer, Franziska; Fischer, Dieter; Klaeger, Franziska; Ivar do Sul, Juliana; Labrenz, Matthias (2020): Microplastics in wastewater treatment: Development of sampling and analysis methods for detection of input quantities into surface waters. Fact sheet 11 of the BMBF research focus „Plastics in the Environment“.

Publikationstyp

Ergebnis

Factsheet 7.2: Mikroplastik im Nahrungsnetz in Gewässern - Analyse von Wirkung und Transfer am Beispiel der Fadenwürmer (Nematoden)

janna.vakili@ecologic.eu — Thu, 06 May 2021 12:42:40 +0000

Factsheet 7.2: Microplastics in the aquatic food web - Impact and transfer analysis based on the example of roundworms (nematodes) janna.vakili@e… Thu, 05/06/2021 - 14:42

Titelbild

Photo: © Hendrik Füser, Bielefeld University, Department of Animal Ecology

Beschreibung

"To assess the ecologic danger posed by microplastics, one must also consider indirect effects in the food web", say Sebastian Höss (Ecossa) and Marie-Theres Rauchschwalbe (Bielefeld University). The researchers from the joint project MikroPlaTaS looked at these effects using nematodes as an example.

Roundworms (nematodes) live in the sediment layer of water bodies and serve as a food source for larger aquatic organisms. Nematodes are capable of absorbing microplastics within a matter of minutes, resulting in these small plastic particles entering the food chain. Insights into the subsequent effects are useful for considering the transfer of microplastics in the food web, as nematodes are a significant food source for organisms in the bottom zone of the water body.

The project partners of the joint project MikroPlaTaS worked in the field, in the laboratory and in semi-outdoor systems (micro- and mesocosms). In this way, impact thresholds and mechanisms were modelled with the help of individual laboratory species of meio- and macrofauna, which could then be tested under realistic conditions for complex organism communities.

The results of the investigations are presented in the second factsheet of the research project. This is available here as a PDF download.

Attachments

Factsheet 7.2 of the BMBF Research Focus Plastics in the Environment.

Joint project

MikroPlaTas

Year

2021

Author

Authors

Sebastian Höss

Marie-Theres Rauchschwalbe

Hendrik Fueser

Walter Traunspurger

Type of Result

factsheets

Citation

Höss, Sebastian; Rauchschwalbe, Marie-Theres; Fueser, Hendrik; Traunspurger, Walter (2021): Microplastics in the aquatic food web: Impact and transfer analysis based on the example of roundworms (nematodes). Fact sheet 7.2 of the BMBF research focus „Plastics in the Environment“.

Tags

Environmental sustainability

Whereabouts

Publikationstyp

Ergebnis

QST1: Vergleichsversuch

janna.vakili@ecologic.eu — Fri, 12 Feb 2021 09:52:50 +0000

Cross-Cutting Topic 1: Analytics and Reference Materials: Comparative test janna.vakili@e… Fri, 02/12/2021 - 10:52

Untertitel

Results

Titelbild

Beschreibung

This comparative test from cross-cutting topic 1 "Analytics and reference materials" classifies different analytical methods for the identification and quantification of microplastics regarding their informative value and to work out the strengths and limitations of the respective methods. The comparative test was intended to provide the pre-requisites for comparing the analytical results of the individual projects within a given framework. No evaluation of the different analytical methods is intended.

Both thermoanalytical and spectroscopic methods were used. It was shown that the different analytical methods for the identification and quantification of microplastics provide comparable results within the respective procedures.

The results of the comparative test are available here as a PDF download.

Attachments

Cross-Cutting Topic 1: Analytics and Reference Materials: Comparative test

Year

2021

Author

Authors

PD Dr. Natalia Ivleva

Prof. Dr. rer. nat. Heinz Sturm

Cordula Witzig

Dr. Nicole Zumbülte

Type of Result

discussion papers & status papers

Tags

Methodology of analyses

Polyethylene terephthalate (PET)

Polymer

Polymer analysis

Raman microspectroscopy

Publikationstyp

InRePlast

Stephan.Guertler — Fri, 01 Mar 2019 09:03:22 +0000

InRePlast Stephan.Guertler Fri, 03/01/2019 - 10:03

Environmental Policy Instruments to Reduce Plastic Pollution of Inland Waters through Drainage Systems

The project aimed to make a significant, transdisciplinary contribution to applied research on the prevention of plastic discharges into water bodies via drainage systems from a behavioural and environmental economics perspective. In four model municipalities, the project recorded the quantity and type of plastics discharged into the drainage systems via wastewater and precipitation water collection in municipal wastewater treatment plants and precipitation drains within one year. The data obtained was then extrapolated for Germany by means of material flow analysis. With regard to regulatory deficits, instruments to reduce plastic inputs were developed in an interplay of legal and behavioural economics analyses. Selected instruments were tested in field experiments in companies and households. On this basis, the project partners developed policy briefs that inform policymakers, practitioners and associations about ways to measure and reduce plastic inputs into the environment.

Main areas of work

Analysis of legal framework conditions
Empirical investigations of plastic discharges into the drainage systems of four model municipalities
Model-based visualisation of the material flows from the considered input sources, namely households, transport routes and companies of the plastics industry in the model municipalities
Development of behaviour-based measures to motivate behavioural changes
Computer simulations of the effects of behaviour-based measures
Evaluation of the effect of measures by means of field experiments

Arbeitspakete

Work packages

WP 1: Inventory of the entry points of plastics into the drainage systems

Contact person

Dr. Marco Breitbarth, Research Institute for Water and Waste Management at RWTH Aachen (FIW), Kackertstraße 15 – 17, 52056 Aachen, e-mail: breitbarth@fiw.rwth-aachen.de

Project partners

City of Aachen, City of Stolberg, Simmerath Municipality, Roetgen Municipality, University of Kassel, Darmstadt University of Applied Sciences

Short description

The aim of this work package was to determine the status quo of plastic discharges into the drainage systems in the four selected model municipalities, which represent different settlement structures. For this purpose, the type and quantity of plastic products as well as their sources from households, industry, traffic and other activities related to wastewater collection and drainage of paved areas were determined.

WP 2: Development of a concept for multi-criteria, behavior-oriented set of instruments

Contact persons

Prof. Dr. Anja Hentschel, Darmstadt University of Applied Sciences, Department of Social Sciences, Professorship for Environmental and Energy Law, Haardtring 100, 64295 Darmstadt, e-mail: anja.hentschel@h-da.de

Dr. Maria Daskalakis, University of Kassel, Department of Economics, Division of Economic Policy, Innovation and Entrepreneurship, Environmental Policy Working Group, Nora-Platiel-Str. 4, 34109 Kassel, e-mail: daskalakis@wirtschaft.uni-kassel.de

Project partners

Prof. Dr. Frank Beckenbach, FIW

Short description

Starting from a behavioural economics analysis of relevant behavioural effects regarding the use of plastics in households and companies and possible approaches to motivate changes in their use as well as an investigation and deficit analysis of the existing legal framework at national and European level, behavioural measures and instruments were identified. Their effects with regard to ecological, social, technical, legal and economic feasibility were assessed. The result was a preliminary set of instruments, which were used as a basis for all further investigations and were adapted if necessary.

WP 3: Empirical analyses of success factors and barriers

Contact persons

Dr. David Hofmann, University of Kassel, Department of Economics, Division of Economic Policy, Innovation and Entrepreneurship, Environmental Policy Working Group, Nora-Platiel-Str. 4, 34109 Kassel, e-mail: dhofmann@uni-kassel.de

Project partners

City of Aachen, City of Stolberg, Simmerath Municipality, Roetgen Municipality, Prof. Dr. Frank Beckenbach, FIW, Darmstadt University of Applied Sciences

Short description

The empirical determination of the success factors and barriers of instruments for the reduction of plastic inputs via the drainage systems was based on the concept of multi-criteria behaviour-oriented instrumentation. The focus of the investigations were the actor groups households and companies. The investigations were preceded by expert discussions. A methodological triangulation was used: semi-structured, guideline-supported in-depth interviews were carried out as well as, in the case of households, a telephone survey and, in the case of households and companies, a field experiment.

WP 4: Material flow models of plastic inputs into canalisation systems and wastewater treatment plants

Contact person

Dr. Marco Breitbarth, Research Institute for Water and Waste Management at RWTH Aachen (FIW), Kackertstraße 15 – 17, 52056 Aachen, e-mail: breitbarth@fiw.rwth-aachen.de

Project partners

University of Kassel, Darmstadt University of Applied Sciences

Short description

Material flow models for plastic discharges of macro- and microplastics from the identified sources into the drainage systems were developed for the four model communities. Based on the model results, the sources and product types were analysed and evaluated with regard to their relevance for the plastic inputs. The data from the municipalities was then extrapolated to the federal level in a general model.

WP 5: Actor-based computer model and simulations for the development of material flows

Contact persons

Project partners

Prof. Dr. Frank Beckenbach, FIW, Darmstadt University of Applied Sciences

Short description

In this work package the design and development of multi-agent systems was carried out, which cover the actor groups households and companies. Based on the actor concept of WP 2, the multi-agent systems map actor-related decision-making processes and determinants of plastics use were linked to the material flow models from WP 4 in a subsequent step. Different legal and behavioural instruments and their material-ecological and economic implications were analysed and evaluated on the basis of different scenarios.

WP 6: Finalisation of the concept of multi-criteria, behaviour-oriented set of instruments

Contact person

Project partners

Prof. Dr. Frank Beckenbach, University of Kassel, FIW

Short description

In parallel to work packages 3 to 5, the concept of multi-criteria behaviour-oriented set of instruments were further specified by including the results of empirical studies and the multi-agent system. For the identified instruments and measures, it was estimated how they could work in practice, what control and enforcement effort they might create for authorities, whether they could be combined in certain areas, and what medium- and long-term effects the regulations could have. The adjustments to the concept were tracked and evaluated through computer simulations.

WP 7: Developing proposals for implementation

Contact persons

Dr. Marco Breitbarth, Research Institute for Water and Waste Management at RWTH Aachen (FIW), Kackertstraße 15 – 17, 52056 Aachen, e-mail: breitbarth@fiw.rwth-aachen.de

Project partner

Prof. Dr. Frank Beckenbach

Short description

The project results were prepared for political and practical implementation. For this purpose, recommendations for action were summarised in the form of policy briefs, which are intended to offer support to various actors for the implementation of the developed instrument packages. The project addressed the federal, state and local levels (legislators and authorities), consumer associations and NGOs as well as companies and associations of the plastics industry in order to facilitate the effective implementation of the measures.

Coordinator

Dr. Maria Daskalakis
University of Kassel, Department of Economics, Division of Economic Policy, Innovation and Entrepreneurship,
Environmental Policy Working Group
Nora-Platiel-Str. 4
34109 Kassel
Phone: +49 561 804-3052
e-mail: daskalakis@wirtschaft.uni-kassel.de

Website

www.inreplast.de

Partner Institutions

Darmstadt University of Applied Sciences, Professorship for Environmental and Energy Law

Research Institute for Water and Waste Management at RWTH Aachen / FiW

Associated Partners

City of Aachen

City of Stolberg

Simmerath Municipality

Roetgen Municipality

Wasserverband Eifel-Ruhr / WVER

BKV GmbH

German Association for Plastics Packaging and Films / IK

PlasticsEurope Germany

Kunststoff-Zentrum SKZ

German Federal Environmental Agency

DHB – Netzwerk Haushalt

BildungsCent e.V.

Prof. Dr. Frank Beckenbach, Cusanus Hochschule, Bernkastel-Kues

Duration Period

January 2019

December 2021

Tags

Sewage treatment plant

Multi-criteria evaluation

Standardization

Strategy on plastics

Plastic littering

Reduction of plastic use

Prevention of plastics

minimization strategies

Regulation

Project sheet

Project-sheet-InRePlast-2019.pdf

Koordinator label

Coordinator

Instrumental Analysis of Microplastics - Benefits and Challenges

Stephan.Guertler — Mon, 09 Jul 2018 08:08:15 +0000

Instrumental Analysis of Microplastics - Benefits and Challenges Stephan.Guertler Mon, 07/09/2018 - 10:08

Titelbild

Beschreibung

There is a high demand for easy, cheap, comparable, and robust methods for microplastic (MP) analysis, due to the ever-increasing public and scientific interest in (micro-) plastic pollution in the environment. Today, a multitude of methodologies for sampling, sample preparation, and analysis of MPs are in use.

This feature article deals with the most prominent detection methods as well as with sampling strategies and sample preparation techniques. Special emphasis is on their benefits and challenges. Thus, spectroscopic methods, coupled with microscopy, require time-consuming sample preparation and extended measurement times, whereas thermo-analytical methods are faster but lack the ability to determine the size distribution in samples.

To that effect, most of the described methods are applicable depending on the defined analytical question.

Further Links

Download article (restricted access)

DOI

https://doi.org/10.1007/s00216-018-1210-8

ISSN

1618-2642

Magazine

Analytical and Bioanalytical Chemistry

Year

2018

Author

Sven Huppertsberg

Thomas Knepper

Publisher

Springer

Type of Result

(scientific) publications (peer-review, essays, book chapters, poster etc.)

Citation

Huppertsberg, Sven & Knepper, Thomas. Instrumental analysis of microplastics—benefits and challenges. Analytical and Bioanalytical Chemistry (2018). https://doi.org/10.1007/s00216-018-1210-8

Tags

Publikationstyp

MicroCatch_Balt

KALEH — Wed, 20 Dec 2017 09:57:04 +0000

MicroCatch_Balt KALEH Wed, 12/20/2017 - 10:57

Investigation of Sinks and Sources of Microplastics from a Typical Catchment Area to the Open Baltic Sea

This project determined sources and sinks of microplastic in the Warnow river basin, as well as relevant dissemination processes on its way to the open Baltic Sea. Separate models were linked so that the resulting model covers the entire river basin including estuary and coastal waters. The linked models served to identify hotspot areas of microplastic entry and to estimate the effects of microplastic reduction measures in parts of the river basin. By converting the models into a handson multitouch table, project participants made interactive, creative learning modules that were presented in the form of a traveling exhibition in communities around the German Baltic coast from Stralsund to Flensburg. Further, MicroCatch_Balt included the examination of anti-fouling paint and extreme weather events as sources and higher organisms as sinks. Based on this, MicroCatch_Balt covered the most important aspects of microplastic contamination of limnic to marine systems in northern Germany, thereby offering interest groups the expertise with which to develop future monitoring and strategies for reduction.

Main areas of work

Sampling in the Warnow river basin and estuary, extraction and identification of microplastics
Modelling of microplastic input into the Warnow system of diffuse and point sources
Development of two multi-media modules for a multi-touch table and organisation of a traveling exhibition

Arbeitspakete

Work packages

WP 1 Sampling of microplastic from the environment

Contact person
PD Dr. habil. Matthias Labrenz, Leibniz Institute for Baltic Sea Research, Environmental Microbiology, Seestraße 15, 18119 Rostock, e-mail: matthias.labrenz@io-warnemuende.de

Project partner
IPF

Short description
In WP 1, environmental samples (water, sediment, soil, benthic and pelagic higher organisms) were collected, processed and identified in the Warnow area. Of particular interest were potential sources such as wastewater treatment plants / sewage separation, drainage ditches, erosion areas, industrially influenced areas as well as extreme events like Hanse Sail, New Year‘s Eve, heavy rain and storm events. Potential sinks, including higher organisms (mussels, worms, fish), beaches and sediments were also sampled. In all samples, the microplastic particles were identified and quantified using spectroscopic methods.

WP 2 Modelling of the Warnow estuary and the catchment area

Contact person
Dipl.-Ing.agr. Peter Kreins, Johann Heinrich von Thünen Institute - Federal Research Institute for Rural Areas, Forestry and Fisheries, Bundesallee 50, 38116 Braunschweig, e-mail: peter.kreins@thuenen.de

Project partner
FZJ, IOW

Short description
By adapting and combining different regional models, spatially high-resolution modelling of landside diffuse and point source of microplastic emissions into the river basin of the Warnow took place. In this way, on the one hand the hotspots of pollution in the Warnow river area were identified and on the other hand the entire landside microplastic entries into coastal waters were quantified.

WP 3 Microplastics Touring Exhibition

Contact person
Dr. Barbara Hentzsch, Leibniz Institute for Baltic Sea Research Warnemünde, Scientific Management and Communication, Seestraße 15, 18119 Rostock, e-mail: barbara.hentzsch@io-warnemuende.de

Project partner
FhIGD

Short description
In WP 3 a traveling exhibition with an interactive multimedia learning module was developed, which presents the project results in the form of animations. The traveling exhibition was shown in Stralsund, Rostock, Hamburg, Kiel, Eckernförde and Flensburg. The respective exhibition openings was accompanied by plenary discussions with representatives of the local environmental authorities and scientists.

WP 4 Project management

Contact person
PD Dr. habil. Matthias Labrenz, Leibniz Institute for Baltic Sea Research, Environmental Microbiology, Seestraße 15, 18119 Rostock, e-mail: matthias.labrenz@io-warnemuende.de

Short description
WP 4 covered project management and ensured efficient and productive execution of the project. The tasks of WP 4 included coordination with the other “Plastics in the Environment” projects PLAWES, PLASTRAT and the BONUS project MICROPOLL, as well as monitoring finances and work results, organising regular project meetings, disseminating project results to the public, and supporting the project manager with regard to internal and external scientific communication.

Coordinator

PD Dr. habil. Matthias Labrenz
Leibniz Institute for Baltic Sea Research Warnemünde / IOW,
Environmental Microbiology
Seestraße 15
18119 Rostock
Phone: +49 381/5197378
e-mail:matthias.labrenz@io-warnemuende.de

Website

https://www.io-warnemuende.de/microcatch-home.html

Partner Institutions

Leibniz Institute of Polymer Research Dresden / IPF

Jülich Research Centre, Institute for Bio- and Geosciences / FZJ-IBG

Johann Heinrich von Thünen Institute - Federal Research Institute for Rural Areas, Forestry and Fisheries / TI-LR

Fraunhofer Institute for Computer Graphics Research IGD Rostock / FhIGD

Duration Period

August 2017

April 2021

Tags

Information and teaching materials

Infraref spectroscopy

Sewage treatment plant

Combined sewar overflows

Project sheet

19_Projektblatt_MicroCatchBalt_ENG_2018.pdf

Koordinator label

Coordinator

PLAWES

KALEH — Wed, 20 Dec 2017 09:29:04 +0000

PLAWES KALEH Wed, 12/20/2017 - 10:29

Microplastic Contamination in the Weser- Wadden Sea – National Park Model System: an Ecosystem-Wide Approach

In PLAWES, the modelling system of the German national park Weser-Wadden Sea was the first large European river basin that was investigated in detail regarding its microplastic pollution. PLAWES conducted a pioneering study of the microplastic contamination from the headwaters to the North Sea (northern Atlantic Ocean) that comprised an interdisciplinary and integrated ecosystem approach and accounted for various point sources (wastewater treatment plants, separation systems) and diffuse sources (drainage, atmosphere) of pollution. The results were integrated into a model for identifying primary transport mechanisms and accumulation zones. The research investigated the effects of microplastics on ecosystems in the Weser-Wadden Sea system by analysing the interaction of microplastic with pathogens in biofilm and aquatic invertebrates. Outcomes of this particularly ecologically relevant aspects were used to estimate the environmental risk of microplastics for the model system, and subsequently made it transferable to other systems. In addition, the results of the analysis became part of new teaching materials in order to provide a knowledge platform for teachers, students, and parents across Europe. PLAWES generated unique data about the effects of microplastics on a large European river basin and its environment. This is significant not only for policymakers and stakeholders but also as a fundament for science-based solutions to address the microplastics problem.

Main areas of work

Microplastics in the Weser-Wadden Sea
Model-based balancing of diffuse and point sources of microplastic entries
Interaction of microplastics with pathogens and biota
Training measures to raise awareness of plastic waste

Arbeitspakete

Work packages

WP 0 Management, communication and dissemination

Contact person
Prof. Dr. Christian Laforsch, University of Bayreuth, Universitätsstraße 30, 95447 Bayreuth, e-mail: christian.laforsch@uni-bayreuth.de

Project partner
AWI

Short description
WP 0 ensured the targeted and efficient support of the consortium with regard to project management, communication and dissemination. WP 0 coordinated both the public relations work and the exploitation of the results achieved. WP 0 continued to coordinate the cooperation of all project partners and was therefore in close contact with all project partners. WP 0 coordinated the harmonisation with the joint research project MicroCatch_Balt with regard to sampling and processing, modelling, public relations, and data storage as well as communication with the other projects.

WP 1 Microplastics in the Weser-Wadden Sea model system

Contact person
Dr. Gunnar Gerdts, Alfred Wegener Institute, Helmholtz Centre for Polar and Marine Research, Kurpromenade, 27498 Helgoland, e-mail: gunnar.gerdts@awi.de

Project partner
UBT, UOld

Short description
The aim of WP 1 was to investigate the entire Weser river system into coastal waters with regard to microplastic pollution. The final determination of the exact sampling points was carried out taking into account the real data required for RAUMISmGROWA- MePhos and "Tidal Model" (WP 3). The entire Weser including the Lower Weser and the Wadden Sea was investigated with regard to exposure to microplastic. Two campaigns were carried out at different seasons with different water conditions on the Weser.

WP 2 Entry points – point sources and diffuse entry

Contact person
Prof. Dr. Andreas Held, University of Bayreuth, BayCEER; second affiliation: Technical University of Berlin, Department of Environmental Chemistry and Air Pollution Control, Straße des 17. Juni 135, 10623 Berlin, e-mail: held@tu-berlin.de

Project partner
AWI

Short description
The aim of WP 2 was an exemplary consideration of the input paths for microplastics by investigation of important point sources such as wastewater treatment plants and separation water sewer systems as well as the diffuse input from drains and atmosphere. For this purpose, selected sampling points in the Weser river basin were characterised taking into account different landscape areas and land use types. The focus lay on quantifying the entry points of microplastics. Sampling was synchronised with the campaigns at the Weser.

WP 3 Model-based accounting of diffuse and point-shaped MP entries

Contact person
Prof. Dr. Frank Wendland, Jülich Research Centre IBG-3, Wilhelm-Johnen-Straße, 52428 Jülich, e-mail: f.wendland@fz-juelich.de

Project partner
TI, NLWKN

Short description
The aim was a spatially resolved quantification of the microplastic emissions from diffuse and point sources and the identification of spatial load centres and accumulation zones within the river basin and estuary. The microplastic entries were modelled from different types of diffuse entry points and point sources. The work was based on the models mGROWA, MEPhos, RAUMIS, as well as a transport modelling considering the estuarine hydro- and sediment dynamics. Within the framework of the project, the model chain was improved in a targeted manner according to microplastic entry modelling in the inland and the further distribution of the microplastics in the lower reaches, estuary and apron.

WP 4 Interaction of microplastic with pathogens and biota

Contact person
Prof. Dr. Jörg Oehlmann, Goethe University Frankfurt, Max-von-Laue-Straße 13, 60438 Frankfurt am Main, e-mail: oehlmann@bio.uni-frankfurt.de

Project partner
AWI, UBT, UOld

Short description
In WP 4, the ecosystem effects of microplastic on the Weser-Wadden Sea model system were described on the basis of the two ecologically relevant aspects "Interaction with pathogens and antimicrobial resistance" and "Interaction with aquatic invertebrates".

Interaction with pathogens and antimicrobial resistance: Since biofilms are sites of increased genetic exchange and increased antimicrobial resistance occurs below wastewater treatment plants, plastics could not only contribute to the dispersion of pathogenic organisms, but also of resistance genes. The consequences of such a transfer were previously unknown. AWI therefore used molecular microbial source tracking techniques (DNA/RNA arrays for the detection of pathogenic bacteria, viruses, protozoa and virulence/resistance genes) to investigate plastic samples from the Weser region. Interaction with aquatic invertebrates: In order to generate exposure data, different mollusk species were applied in situ in the Weser, the tidal area and the Wadden Sea. Absorbed microplastic was examined in the digestive tract and in tissue samples and confirmed in parallel by pyrolysis-GC-MS and spectroscopic methods. Historical mussel samples (since 1986) from the Federal Environmental Specimen Bank (UBA) were examined using pyrolysis-GC-MS. The chronic toxicity of microplastic is characterised in laboratory experiments with mussels and worms. Different polymers were conditioned in situ and toxicologically characterised in chronic exposure experiments.

WP 5 Training measures to raise awareness of plastic waste

Contact person
Prof. Dr. Franz X. Bogner, University of Bayreuth, Didactics of Biology, Universitätsstraße 30, 95447 Bayreuth, e-mail: franz.bogner@uni-bayreuth.de

Project partner
AWI, UOld

Short description
In addition to the ethical assessment skills of students, WP 5 incorporated existing individual environmental knowledge. Innovative teaching materials with a sound reference to everyday life were evaluated for a holistic understanding regarding the burden of plastics in the model system and disseminated via an Internet teaching/learning portal. Within the work package, UBT provided a handbook for teachers and "public relations workers".

Coordinator

Prof. Dr. Christian Laforsch
University of Bayreuth
Chair of Animal Ecology I / UBT
Universitätsstraße 30
95447 Bayreuth
Phone: +49 921 / 55-2651
e-mail: christian.laforsch@uni-bayreuth.de

Dr. Gunnar Gerdts
Alfred Wegener Institute
Helmholtz Centre for Polar and Marine Research (AWI)
Kurpromenade
27498 Helgoland
Phone: +49 4725 / 819-3245
e-mail: gunnar.gerdts@awi.de

Website

http://www.bayceer.uni-bayreuth.de/PLAWES/en/

Partner Institutions

Coast Research Centre at the Lower Saxony State Enterprise for Water Management, Coastal Protection and Nature Conservation / NLWKN

Jülich Research Centre / FZJ

Goethe University Frankfurt / GU

Johann Heinrich von Thünen Institute - Federal Research Institute for Rural Areas, Forestry and Fisheries / TI-LR

Carl von Ossietzky University of Oldenburg, Institute of Chemistry and Biology of the Sea / UOld

Duration Period

September 2017

April 2021

Tags

Sewage

Methodology of analyses

Information and teaching materials

Infrared

Infraref spectroscopy

Sewage treatment plant

Sewage sludge

Municipality

Communication strategy

Combined sewar overflows

Prevention of plastics

Polyamide (PA)

Polyester

Polyethylene (PE)

High density polyethylene PE-HD

Polyethylene terephthalate (PET)

Polyvinyl chloride (PVC)

sampling

Sample purification

Pyrolysis GC

Raman microspectroscopy

Environmental sustainability

Scanning electron microscopy

Plasticiser

Project sheet

18_Projektblatt_PLAWES_ENG_2018.pdf

Koordinator label

Coordinator

MikroPlaTaS

KALEH — Wed, 20 Dec 2017 08:53:43 +0000

MikroPlaTas KALEH Wed, 12/20/2017 - 09:53

Microplastics in Dams and Reservoirs: Sedimentation, Spread, Effects

The spread of microplastics in rivers showed that along a given waterway there are sources as well as sinks. Thus, dams and reservoirs constitute important but until now hardly investigated parts of a water system that serve as examples for risk vs. usefulness of sedimentation of microplastics. Biofilms, which grow on microplastics, have a special significance for their transport and sedimentation. The goals of this project were (I) to identify and characterise microplastic in water and sediment, (II) to understand how biofilms form on plastic and how sedimentation occurs on these grown-over particles, (III) to record how microplastics affect and are taken up by individual organisms as well as by entire communities in model ecosystems, and (IV) to synthesise the scientific results and draft practical recommendations based on them. This synthesis emphasised identifying pathways to eliminate microplastics and to derive practical measures and risk assessments together with the project partners.

Main areas of work

Distribution and sedimentation of microplastics and fauna in situ
Characterisation of microplastics with regard to biofilm communities and sedimentation mechanisms
Direct effects of microplastic on invertebrate species and complex biocenoses
Influence of plastics on the food quality of biofilms for Grazer

Arbeitspakete

Work packages

WP 1 Survey plastics and meio- and microfauna in dams and reservoirs

Contact person
PD Dr. Katrin Wendt-Potthoff, UFZ, Department of Lake Research, Brückstraße 3a, 39114 Magdeburg, e-mail: katrin.wendt-potthoff@ufz.de

Project partner
WWU, Bielefeld University

Short description
The aim was to estimate the contamination of various dammed waters with microplastics, to identify the relevant polymers and to determine the respective typical macro- and meiofauna. Different service water reservoirs (e.g. Bautzen in Saxony) as well as the dammed Ems, the Lippe and the former Rieselfelder Münster in North Rhine-Westphalia were adhesively investigated.

WP 2 In situ experiments on sedimentation rates and settlement

Contact person
PD Dr. Katrin Wendt-Potthoff, UFZ, Department of Lake Research, Brückstraße 3a, 39114 Magdeburg, e-mail: katrin.wendt-potthoff@ufz.de

Project partner
WWU, Bielefeld University

Short description
The aim was to determine field sedimentation rates in the course of a year with regard to total mass and microplastics. For this purpose, sediment traps were applied to the deepest points of the waters, at minimum, and evaluated monthly with regard to the total mass of plastics and organisms of the meiofauna. As a result, a relationship is established between plastic load in the water column, total sedimentation rate and plastic sedimentation rate.

WP 3 Characterisation of biofilms on different polymers

Contact person
Prof. Dr. Bodo Philipp, University of Münster, Institute of Molecular Microbiology and Biotechnology, Corrensstraße 3, 48149 Münster, e-mail: bodo.philipp@uni-muenster.de

Project partner
UFZ, UP, Bielefeld University

Short description
In this work package, the microbial communities on plastic particles were examined with regard to taxonomic composition and function in order to derive hypotheses on processes at the sites that can be checked in WPs 4 – 6. Particular attention was paid to whether there is a characteristic microflora on microplastic particles and whether individual types of plastic differ. Furthermore, mechanisms of biofilm formation on microplastic particles were explained. Cultivation-dependent and -independent investigations were carried out with samples from WP 1 and WP 2 and later with mesocosmic samples (WP 5). A collection of strains is to be generated in the first project year so that it can be used for WP 5 and WP 6.

WP 4 Influence of biofilm colonisation, light and redox processes on microplastic sedimentation

Contact person
PD Dr. Katrin Wendt-Potthoff, UFZ, Department of Lake Research, Brückstraße 3a, 39114 Magdeburg, e-mail:katrin.wendt-potthoff@ufz.de

Project partner
WWU, Bielefeld University

Short description
Experiments under controlled conditions determined how light and redox ratios (concentration of O2 and iron) influence the sedimentation of plastic particles either directly or by controlling colonisation. The influence of these factors on sedimentation was studied to simulate the transition from pelagic to benthic habitat. To what extent light or darkness and oxic or anoxic conditions per se, but also their change, can control the sinking behaviour of plastic particles was determined.

WP 5 Direct effect of plastic particles on invertebrates

Contact person
Prof. Dr. Walter Traunspurger, Bielefeld University, Department of Animal Ecology, Konsequenz 45, 33615 Bielefeld, e-mail: traunspurger@uni-bielefeld.de

Project partner
WWU, UP, Ecossa, Mesocosm

Short description
The uptake and effect of microplastics for aquatic organisms was tested in experimental systems (single-species to model ecosystems) to assess risks for pelagic and benthic fauna. A harmful effect in the organism requires an uptake into the body, either through the ingestion of the particles themselves or through transfer in the food chain (biomagnification). In case of harmful effects, indirect effects (top-down, bottom-up) can occur and thus affect organisms not directly affected by microplastic. In order to evaluate the food web as fully as possible, experiments with increasing ecological complexity and relevance were carried out for pelagic and benthic invertebrates to elucidate the effect on organisms, populations and communities and to reduce the interpretation gap between laboratory and field results.

WP 6 Influence of plastics on the food quality of biofilm for meio and macro grazers

Contact person
Dr. Friederike Gabel, University of Münster, Institute of Landscape Ecology, Heisenbergstraße 2, 48149 Münster, e-mail: gabelf@uni-muenster.de

Project partner
UP, Bielefeld University, UFZ

Short description
The aim of this WP was to identify indirect effects of microplastic on meio and macrofauna organisms by influencing the nutritional basis. Biofilms (especially bacteria, fungi, protozoa) form an important food basis for meio and macrofauna in waters. The quality of these biofilms can therefore have a significant influence on the composition and vitality of the organisms grazing them. For grazing experiments, macro invertebrates were offered different overgrown plastic strips for grazing. Ingestion and excretion rates, growth and, in the case of snails, the reproduction of organisms were investigated.

WP 7 Coordination, public relations, knowledge transfer

Contact person
Dr. Friederike Gabel, University of Münster, Institute of Landscape Ecology, Heisenbergstraße 2, 48149 Münster, e-mail: gabelf@uni-muenster.de

PD Dr. Katrin Wendt-Potthoff, UFZ, Department of Lake Research, Brückstraße 3a, 39114 Magdeburg, e-mail: katrin.wendt-potthoff@ufz.de

Project partner

UP, Bielefeld University, Ecossa, Mesocosm

Short description
The aim was to communicate project results to specific target groups both within the consortium and to the general public (children, students, authorities and scientists). The practical partners (The State Reservoir Administration of Saxony, Lower Water and Landscape Authority of the City of Hamm, Academy of nature and Environmental Protection NRW) played an important role here. The multiplier effect of the addressed target groups promoted the project results and the topic of plastics in the environment and this sensitisation created a broader acceptance for the recommendations for action that arose from the research focus.

Coordinator

PD Dr. Katrin Wendt-Potthoff
Helmholtz Centre for Environmental Research – UFZ,
Department of Lake Research
Brückstraße 3a
39114 Magdeburg
Phone: +49 391 8109810
e-mail: katrin.wendt-potthoff@ufz.de

Website

https://www.uni-muenster.de/Mikroplatas/en/index.html

Partner Institutions

University of Münster / WWU

University of Potsdam / UP

Bielefeld University

Ecossa

Institute for Water Protection Mesocosm GmbH

Duration Period

January 2018

September 2021

Tags

Information and teaching materials

Polyethylene terephthalate (PET)

Polyvinyl chloride (PVC)

Project sheet

16_Projektblatt_MicroPlaTas_ENG_2018.pdf

Koordinator label

Coordinator

EmiStop

KALEH — Tue, 19 Dec 2017 16:41:32 +0000

EmiStop KALEH Tue, 12/19/2017 - 17:41

Identification of Industrial Plastic Emissions by Means of Innovative Detection Methods and Technology Development to Prevent the Input into the Environment via the Wastewater Pathway

This project systematically detected emissions of plastics into wastewater from relevant industries. Emissions levels were analysed along all points of the value chain (production, transport, processing, and cleaning of synthetic materials).

The goal was to select wastewater treatment technologies that optimise the reduction of emissions of plastics for the respective value chain. The project evaluated existing technologies for separating particles, investigated deposition rates, and developed approaches for technical optimisation. Optimisation also includes technological developments such as flocculants. Researchers conducted tests in both laboratory and pilot project settings – selected large scale technical wastewater treatment plants were investigated at industrial facilities.

Due to the existing analytical uncertainties, the following detection methods were used to evaluate the existing and developed technologies:

Dynamic differential calometry for qualification and quantification (concentrations)
Raman spectroscopy for qualification and quantification (particle numbers)
Correlations of the plastic concentrations to routine water chemical analyses (for a retrospective estimation of the plastic loads)
Tracer test with magnetic plastic particles (simple and reliable quantification in large dilutions) for balancing in laboratory and pilot tests

Apart from the technical aspects, the focus of this project was also on socio-economic aspects. Thus, measures to prevent economic losses and retain value were reviewed together with the associated industrial enterprises and evaluated with partners from the scientific community and other interest groups.

Main areas of work

Standardisation of sampling and sample preparation for industrial wastewater (in alignment with Plastik-Net and other joint research projects)
Quantitative and qualitative measurement of plastic concentrations in industrial wastewater using Raman spectroscopy and dynamic differential calorimetry
Extended data collection at the sampled industrial waste water treatment plants for the derivation of the plastic loads and testing of a correlation between the measurement results and routine water chemical analyses
Development of magnetic plastic particles in the micrometre range with the physical properties of relevant types of plastic
Development of a tracer test with magnetic plastic particles
Assessment of technologies for particle separation with regard to the retention of (micro-) plastic particles
Optimisation of particle separation technologies
Development of flocculants for the targeted improvement of the retention of individual types of plastics and their mixtures
Delphi surveys of industry and sector associations as well as of politics and science to identify perceived risks and obstacles as well as opportunities and the willingness to participate
Multi-criteria analysis for the development of weighted, ecological and socio-economic criteria for the sustainability assessment of the project results

Arbeitspakete

Work packages

WP 1 Development of analytical methods for plastic particles

Contact persons
Prof. Dr. Jutta Kerpen, RheinMain University, Institute for Environmental and Process Engineering, Department of Wastewater Treatment, Am Brückweg 26, 65428 Rüsselsheim, e-mail: jutta.kerpen@hs-rm.de

Prof. Dr. Susanne Lackner, Technical University of Darmstadt, Institute IWAR, Department of Wastewater Engineering, Franziska-Braun-Straße 7, 64287 Darmstadt, e-mail: s.lackner@iwar.tu-darmstadt.de

Prof. Dr.-Ing. Markus Engelhart, Technical University of Darmstadt, Institute IWAR, Department of Wastewater Technology, Franziska-Braun-Straße 7, 64287 Darmstadt, e-mail: m.engelhart@iwar.tudarmstadt.de

Project partner
EnviroChemie

Short description
A routinely applicable sampling and sample preparation procedure were developed in order to create a uniform and comparable database for industrial wastewater. For the subsequent qualification and quantification of microplastics in (industrial) wastewater samples, the methods of dynamic differential calorimetry and Raman spectroscopy were adapted to industrial wastewater. The respective analysis results were compared with standardised routine measurements and operational self-analysis to determine correlations.

WP 2 Tracer test

Contact persons
Prof. Dr. Susanne Lackner, Technical University of Darmstadt, Institute IWAR, Department of Wastewater Engineering, Franziska-Braun-Straße 7, 64287 Darmstadt, e-mail: s.lackner@iwar.tu-darmstadt.de

Dr. Kyriakos Eslahian, BS-Partikel GmbH, Nestléstr. 41, 55120 Mainz, e-mail: eslahian@bs-partikel.de

Short description
In order to balance individual process technologies for plastic particle retention in real water matrices, a method for the quantification of magnetic plastic particles by means of magnetic susceptibility scales was established. For this purpose, particles in the size range from 1 μm to 300 μm were synthesised with the greatest possible magnetic susceptibility, which imitate the morphologies and chemical properties of environmental plastic particles.

Furthermore, a continuous method for the production of these particles was established in order to ensure the best possible reproducibility and scalability for subsequent applications.

WP 3 Identification of industrial entry points

Prof. Dr. Susanne Lackner, Technical University of Darmstadt, Institute IWAR, Department of Wastewater Engineering, Franziska-Braun-Straße 7, 64287 Darmstadt, e-mail: s.lackner@iwar.tu-darmstadt.de

Project partner
EnviroChemie, inter 3

Short description
The entry points of microplastics from industrial wastewater into surface waters were determined by uniform characterisation and quantification of the plastic emissions of individual industrial plants. The evaluation of plastic emissions on the basis of mass flows, variations and production information with key figure system and balance tools, hotspots and temporal variations of the particle input were identified.

WP 4 Balancing of technical systems

Contact persons

Dr.-Ing. Eva Bitter, EnviroChemie GmbH, F&E, In den Leppsteinswiesen 9, 64380 Rossdorf, e-mail: eva.bitter@envirochemie.com

Project partner

TU-AW, inter3, HSRM

Short description
In laboratory and pilot tests, various process techniques (filtration in various filter units such as membrane plants, double-layer filters, cloth filters; flocculation in combination with filtration, flotation or sedimentation) were evaluated with regard to plastic particle removal. For this purpose, the tracer particles developed in WP 2 were used, which enable the use of synthetic and real industrial waste water. Furthermore, the existing industrial process technology was evaluated at different industrial sites and optimised with regard to the separation of plastic particles.

WP 5 Optimisation of plastic retention

Contact persons
Dr.-Ing. Eva Bitter, EnviroChemie GmbH, F&E, In den Leppsteinswiesen 9, 64380 Rossdorf, e-mail: eva.bitter@envirochemie.com

Project partner
TU-AW

Short description
Based on the results of WP 4, the pilot plants were adapted by specific design changes (e.g. flow control, sludge removal, conveyor technology) and the success of these optimisations was evaluated in further balancing experiments. For the industries considered, in addition to constructive optimisation of process engineering, production-integrated measures to reduce plastic emissions were derived. The production information collected in WP 3 served as the basis for this.

WP 6 Development of flocculants for plastics sorts

Contact persons
Dr.-Ing. Eva Bitter, EnviroChemie GmbH, F&E, In den Leppsteinswiesen 9, 64380 Rossdorf, e-mail: eva.bitter@envirochemie.com

Project partner
TU-AT, TU-AW

Short description
In experiments with beakers, individual polymers for the targeted flocculation of particles of different types of plastic in the size range from 10 to 300 μm were tested. The results were then used to test specific blends of polymers to produce the most stable flakes of particles of individual plastic types. With these results, the tests and developments were extended to mixtures of different types of plastics.

The laboratory test results were then supplemented by pilot tests using tracer particles developed in WP 2.

WP 7 Risk and potential analysis

Contact person
Dipl.-Ing. Wolf Raber, inter 3 GmbH - Institute for Resource Management, Otto-Suhr-Allee 59, 10585 Berlin, e-mail: raber@inter3.de

Project partner
TU-AT, TU-AW, EnviroChemie, HSRM, BS-Partikel

Short description
To maximise the broad application of the EmiStop optimisation approaches and avoidance strategies, the risks and potentials were identified from the perspective of the key actors, evaluated and fed into the project at an early degree of technology maturity. Furthermore, an expert-supported set of sociopolitical, economic, and ecological evaluation criteria and a meaningful set of indicators were derived in order to analyse and evaluate the multicriterial optimisation approaches and avoidance strategies and in a next step measures for implementation and diffusion.

WP 8 Management and communication

Contact persons
Dr.-Ing. Eva Bitter, EnviroChemie GmbH, F&E, In den Leppsteinswiesen 9, 64380 Rossdorf, e-mail: eva.bitter@envirochemie.com Dr. Anja Steglich, inter 3 GmbH - Institute for Resource Management, 10585 Berlin, e-mail: steglich@inter3.de

Project partner
TU-AT, TU-AW, HSRM, BS-Partikel

Short description
In order to disseminate and implement the project results, industrial companies were actively involved and dialogue is carried out with experts from relevant industry associations (e.g. PlasticsEurope e.V., IK Industrievereinigung Plastikverpackungen e.V., GKV Gesamtverband Plastikverarbeitende Industrie e.V.). The collaboration was commissioned to a) develop the results into a consensual overall perspective, b) prepare these into action-oriented and implementable guidelines and c) make them available via established channels and multipliers, e.g. the Responsible Care Initiative of the chemical industry.

Coordinator

Dr.-Ing. Eva Bitter
EnviroChemie GmbH
In den Leppsteinswiesen 9
64380 Rossdorf
Phone: +49 6154-6998-57
e-mail: eva.bitter@envirochemie.com

Website

http://www.emistop.de/page8.html

Partner Institutions

Technical University of Darmstadt, Institute IWAR, Department of Wastewater Engineering

Technical University of Darmstadt, Institute IWAR, Department of Wastewater Technology

RheinMain University, Institute for Environmental and Process Engineering / HSRM

inter 3 GmbH-Institute for Resource Management

BS-Partikel GmbH

Duration Period

January 2018